Triphenylphosphine 三苯基膦

CAS 603-35-0 MFCD00003043

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产品品牌/编号/名称 纯度规格 包装 价格和现货
INFI H58312
Triphenylphosphine 三苯基膦
99% 25g 40
LN-CN
中国国内现货 96-99 %
INFI H58312
Triphenylphosphine 三苯基膦
99% 100g 70
LN-CN
中国国内现货 96-99 %
INFI H58312
Triphenylphosphine 三苯基膦
99% 500g 130
LN-CN
中国国内现货 96-99 %
Innochem T8500
98% 500g 300
99
Innochem A37091
Triphenylphosphine
98% 25g 48
BJ-CN
中国国内现货 96-99 %
Innochem A37091
Triphenylphosphine
98% 100g 52
BJ-CN
中国国内现货 96-99 %
Innochem A37091
Triphenylphosphine
98% 250g 115
BJ-CN
中国国内现货 96-99 %
Innochem A37091
Triphenylphosphine
98% 500g 225
BJ-CN
中国国内现货 96-99 %
Innochem A37091
Triphenylphosphine
98% 10kg 2,300
96-99 %
Innochem A37091
Triphenylphosphine
98% 20kg -
96-99 %
Purest P58412
Triphenylphosphine 三苯基膦
AR 100g 48
Innochem I01615
4kg -
Innochem I02701
25kg -
TCI T0519
Triphenylphosphine >
>95.0%(T) 25g 97
SH-CN BJ-CN TK-JP
中国国内现货 99
TCI T0519
Triphenylphosphine >
>95.0%(T) 100g 240
BJ-CN
中国国内现货 99
TCI T0519
Triphenylphosphine >
>95.0%(T) 500g 380
SH-CN BJ-CN TK-JP
中国国内现货 99
Alfa A14089
Triphenylphosphine, flake, 99%
99% 250g 647
SH-CN BJ-CN CN
中国国内现货 99
Alfa A14089
Triphenylphosphine, flake, 99%
99% 1000g 1,989
BJ-CN CN
中国国内现货 99
Alfa A14089
Triphenylphosphine, flake, 99%
99% 5000g 4,737
SH-CN BJ-CN CN
中国国内现货 99
Alfa L02502
Triphenylphosphine, powder, 99%
99% 50g 273
SH-CN BJ-CN CN
中国国内现货 99
Alfa L02502
Triphenylphosphine, powder, 99%
99% 250g 654
SH-CN BJ-CN CN
中国国内现货 99
Alfa L02502
Triphenylphosphine, powder, 99%
99% 1000g 2,268
SH-CN BJ-CN
中国国内现货 99
Alfa 014112
99+% 25g 180
BJ-CN
中国国内现货 99
Alfa 014112
99+% 100g 401
BJ-CN
中国国内现货 99
Alfa 014112
99+% 500g 1,325
BJ-CN
中国国内现货 99
J&K 993263
Triphenylphosphine, 99%
99% 25g 74
96-99 %
Acros 14042
Triphenylphosphine, 99%
25g 217
SH-CN BJ-CN CN
中国国内现货 99
Acros 14042
Triphenylphosphine, 99%
250g 653
BJ-CN CN
中国国内现货 99
Acros 14042
Triphenylphosphine, 99%
1kg 688
BJ-CN CN
中国国内现货 99
Acros 14042
Triphenylphosphine, 99%
5kg 7,331
99
Apollo OR9088
Triphenylphosphine
50g 550
0
SIAL T84409
Triphenylphosphine 三苯基瞵
99% 1g 117
99
SIAL T84409
Triphenylphosphine 三苯基瞵
99% 25g 111
SH
中国国内现货 99
SIAL T84409
Triphenylphosphine 三苯基瞵
99% 100g 180
SH
中国国内现货 99
SIAL 93092
Triphenylphosphine 三苯基瞵
>=95.0% (GC) 250g 776
99
SIAL 93092
Triphenylphosphine 三苯基瞵
>=95.0% (GC) 1kg 2,176
99
Energy-chemical W610007
Triphenylphosphine 三苯基膦
98% 25g 50
CN-BJ CN-SH
中国国内现货 99
Energy-chemical W610007
Triphenylphosphine 三苯基膦
98% 100g 65
CN-BJ CN-SH
中国国内现货 99
Energy-chemical W610007
Triphenylphosphine 三苯基膦
98% 500g 168
CN-BJ CN-SH
中国国内现货 99
Energy-chemical W610007
Triphenylphosphine 三苯基膦
98% 5kg 1,280
CN-SH
中国国内现货 99
Energy-chemical W610007
Triphenylphosphine 三苯基膦
98% 25kg 4,000
99
Shao Yuan SY002471
Triphenylphosphine 三苯基膦
97+% 100g 116
SH-CN
中国国内现货 99
Shao Yuan SY002471
Triphenylphosphine 三苯基膦
97+% 500g 226
SH-CN
中国国内现货 99
Acros 140422500
99% 250g 1,009
BJ-CN
中国国内现货 99
TRC T808975
Triphenylphosphine
100g 715
0
TRC T808975
Triphenylphosphine
250g 1,045
0
TRC T808975
Triphenylphosphine
500g 1,250
0
Aladdin T104475
Triphenylphosphine 三苯基膦
>99.0%(GC) 25g 49
CN-SH
中国国内现货 99
Aladdin T104475
Triphenylphosphine 三苯基膦
>99.0%(GC) 100g 56
CN-SH
中国国内现货 99
Aladdin T104475
Triphenylphosphine 三苯基膦
>99.0%(GC) 500g 167
CN-SH
中国国内现货 99
Aladdin T104475
Triphenylphosphine 三苯基膦
>99.0%(GC) 2.5kg 999
CN-SH
中国国内现货 99
Aladdin T104478
Triphenylphosphine 三苯基膦
≥95% 100g 59
CN-SH
中国国内现货 0
Aladdin T104478
Triphenylphosphine 三苯基膦
≥95% 500g 199
CN-SH
中国国内现货 0
Adamas 69212A
99%+ 25g 45
BJ-CN CN
中国国内现货 99
Adamas 69212B
99%+ 100g 60
SH-CN BJ-CN CN
中国国内现货 99
Adamas 69212C
99%+ 250g 88
SH-CN BJ-CN CN
中国国内现货 99
Strem 15-6700
Triphenylphosphine, 99%
99% 100g 315
99
Strem 15-6700
Triphenylphosphine, 99%
99% 500g 1,176
99
Strem 15-6700
Triphenylphosphine, 99%
99% 2kg 2,996
99
SIAL 93092-1KG
>=95.0% (GC) purum, >=95.0% (GC) 1kg 2,176
0
SIAL 93092-250G
>=95.0% (GC) purum, >=95.0% (GC) 250g 776
0
SIAL T84409-100G
99% ReagentPlus(R), 99% 100g 199
99
SIAL T84409-1G
99% ReagentPlus(R), 99% 1g 117
99
SIAL T84409-1KG
99% ReagentPlus(R), 99% 1kg 1,832
99
SIAL T84409-25G
99% ReagentPlus(R), 99% 25g 123
99
SIAL T84409-500G
99% ReagentPlus(R), 99% 500g 971
99
HY Y18824
Triphenylphosphine 三苯基膦
99% 25g -
99
HY Y18824
Triphenylphosphine 三苯基膦
99% 100g -
99
HY Y18824
Triphenylphosphine 三苯基膦
99% 500g -
99
HY Y18824
Triphenylphosphine 三苯基膦
99% 1kg -
99
Aldrich 93092
250g 776
Aldrich 93092
1kg 2,176
Aldrich T84409
1g 117
Aldrich T84409
25g 123
Aldrich T84409
100g 199
Aldrich T84409
500g 971
Aldrich T84409
1kg 1,832
3A A11941
Triphenylphosphine 三苯基膦
99% 100g -
96-99 %
3A A11941
Triphenylphosphine 三苯基膦
99% 500g -
96-99 %
Aladdin T104478-500g
500g 199
BJ-CN
中国国内现货
Aladdin T104478-100g
100g 59
BJ-CN
中国国内现货
Aladdin T104475-500g
500g 167
BJ-CN
中国国内现货
Aladdin T104475-2.5kg
2.5kg 999
BJ-CN
中国国内现货
Aladdin T104475-100g
100g 56
BJ-CN
中国国内现货
Acros 140420250
25g 335
BJ-CN
中国国内现货
Acros 140420010
1kg 1,063
BJ-CN
中国国内现货
Acros 140420050
5kg 7,934
BJ-CN
中国国内现货
Aladdin T104475-25g
25g 49
BJ-CN
中国国内现货
Amethyst 563925
Triphenylphosphine, 99%
99% 25g 49
HB
中国国内现货 96-99 %
Amethyst 563925
Triphenylphosphine, 99%
99% 250g 91
HB SH
中国国内现货 96-99 %
Amethyst 563925
Triphenylphosphine, 99%
99% 1kg 301
SH
中国国内现货 96-99 %

分类

  • {SNA} Catalysis and Inorganic Chemistry, Chemical Synthesis, Phosphine Compounds, Phosphine Ligands
  • {SNA} Basic Phosphine Ligands, Catalysis and Inorganic Chemistry, Chemical Synthesis, Cross-Coupling, Phosphine Compounds, Phosphine Ligands
  • {Chemicalbook} 农药中间体: 杀虫剂中间体: 有机磷类杀虫剂

产品应用

  • 用于有机合成,聚合引发剂,抗菌素类药物氯洁霉素的原料,有机微量分析测定磷的标准样品。

相关文献及参考

  • Azides can be converted selectively to amines, in the presence of ester, epoxide or nitro groups, by reduction to iminophosphoranes (Staudinger reaction), followed by hydrolysis. For reviews, see: Tetrahedron, 37, 437 (1981); 48, 1353 (1992):
  • Finds widespread use as a complexing agent with transition metals, either in the preparation of stable complexes, or as an additive in metal-promoted reactions. See also Tri(o-tolyl)­phosphine, A12093 and Tri(2-furyl)­phosphine, L13329.
  • For use in peptide and other coupling reactions, see 2,2'-Dipyridyl­ disulfide, A11118.
  • In suitable circumstances, the iminophosphorane may undergo intramolecular aza-Wittig reaction: Tetrahedron, 45, 6375 (1989):
  • Reviews: Aza-Wittig reaction in heterocyclic synthesis: Org. Prep. Proced. Int., 24, 209 (1992); Iminophosphoranes as building blocks for the preparation of N-containing heterocycles: Synthesis, 1197 (1994).
  • Merck: 14,9743 Beilstein:16,759
  • Merck: 14,9743
  • For use in the Mitsunobu reaction for conversion of alcohols to alkylating agents, see N-Guanyl­urea sulfate, A19106, and Diisopropyl­ azodicarboxyl­ate, L10386. See also 1,2-Bis(diphenyl­phosphino)­ethane, A11419.

安全信息

Signal word
GHS Symbol
WGK Germany2
Safety Statements
  • S24 Avoid contact with skin 避免皮肤接触;
  • S45 In case of accident or if you feel unwell seek medical advice immediately (show the label where possible) 发生事故时或感觉不适时,立即求医(可能时出示标签);
  • S37 Wear suitable gloves 戴适当手套;
  • S22 Do not breathe dust 不要吸入粉尘;
  • S36/37 Wear suitable protective clothing and gloves 穿戴适当的防护服和手套;
  • S36/37/39 Wear suitable protective clothing, gloves and eye/face protection 穿戴适当的防护服、手套和眼睛/面保护;
  • S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 眼睛接触后,立即用大量水冲洗并征求医生意见;
  • S60 This material and its container must be disposed of as hazardous waste 该物质及其容器必须作为危险废物处置;
  • S61 Avoid release to the environment. Refer to special instructions/safety data sheet 避免释放到环境中,参考特别指示/安全收据说明书;
Risk Statements
  • R48/20/22
  • R53 May cause long-term adverse effects in the aquatic environment 对水生环境有长期的有害作用
  • R43 May cause sensitisation by skin contact 皮肤接触会产生过敏反应
  • R22 Harmful if swallowed 吞咽有害
Precautionary statements
  • P362 Take off contaminated clothing and wash before reuse. 脱掉污染的衣服,清洗后方可重新使用
  • P264 Wash hands thoroughly after handling. 处理后要彻底洗净双手。
  • P271 Use only outdoors or in a well-ventilated area.? 只能在室外或通风良好的地方使用。
  • P261305+351+338
  • P280 Wear protective gloves/protective clothing/eye protection/face protection. 戴防护手套/防护服/眼睛的保护物/面部保护物。
  • P332+313 IF SKIN irritation occurs: Get medical advice/attention. 如果发生皮肤刺激:获取医疗咨询/就医。
  • P260 Do not breathe dust/fume/gas/mist/vapours/spray. 不要吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
  • P501 Dispose of contents/container to..… 处理内容物/容器.....
  • P314 Get medical advice/attention if you feel unwell. 获取医疗咨询/就医,如果你觉得不舒服
  • P301+312+330
  • P302+350 IF ON SKIN: Gently wash with plenty of soap and water. 如果在皮肤上:轻轻地用大量肥皂和水清洗
  • P337+313 IF eye irritation persists: Get medical advice/attention. 如果眼睛刺激持续:获取医疗咨询/就医。
  • P403+233 Store in a well-ventilated place. Keep container tightly closed. 存放在通风良好的地方。保持容器密闭。
Hazard statements
  • H302+332
  • H413 Maycauselonglastingharmfuleffectstoaquaticlife 可能对水生生物造成长期持续有害影响。
  • H317 May cause an allergic skin reaction 可能导致皮肤过敏
  • H302 Harmful if swallowed 吞食有害
  • H373 May causes damage to organs through prolonged or repeated exposure 长期或频繁接触可能会损伤器官
Personal Protective Equipment
  • dust mask type N95 (US), Eyeshields, Faceshields, Gloves
RTECSSZ3500000
Hazard Codes
  • Xn
Storage condition
  • 充氮密封保存。
  • Store at RT.
  • 充氮密封避光保存。
UN Number
Warnings
  • 危化品目录(2015)
TYPE OF TEST            : LC50 - Lethal concentration, 50 percent kill
ROUTE OF EXPOSURE       : Inhalation
SPECIES OBSERVED        : Rodent - rat
DOSE/DURATION           : 1135 ppm/4H
TOXIC EFFECTS :
   Sense Organs and Special Senses (Eye) - lacrimation
   Lungs, Thorax, or Respiration - dyspnea
   Nutritional and Gross Metabolic - weight loss or decreased weight gain
REFERENCE :
   AIHAM* Annual Meeting of American Industrial Hygiene Association.  (Akron,
   OH)  For publisher information, see AIHAAP.  Volume(issue)/page/year:
   -,-,1969

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Subcutaneous
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 3 gm/kg
TOXIC EFFECTS :
   Behavioral - convulsions or effect on seizure threshold
REFERENCE :
   EPASR* United States Environmental Protection Agency, Office of Pesticides
   and Toxic Substances. (U.S. Environmental Protection Agency, 401 M St., SW,
   Washington, DC 20460)  History unknown.  Volume(issue)/page/year:
   8EHQ-0384-0014

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Mammal - dog
DOSE/DURATION           : >500 mg/kg
TOXIC EFFECTS :
   Behavioral - convulsions or effect on seizure threshold
   Lungs, Thorax, or Respiration - dyspnea
   Gastrointestinal - changes in structure or function of salivary glands
REFERENCE :
   NTIS** National Technical Information Service.  (Springfield, VA 22161)
   Formerly U.S. Clearinghouse for Scientific & Tech

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - rat
DOSE/DURATION           : 700 mg/kg
TOXIC EFFECTS :
   Behavioral - convulsions or effect on seizure threshold
REFERENCE :
   EPASR* United States Environmental Protection Agency, Office of Pesticides
   and Toxic Subs

Packing GroupIII

其他信息

  • 方法二:溴苯经格式反应后,用三氯化磷进行膦化反应得到三苯膦。
  • 用途一:用于有机合成,也用作聚合引发剂、抗菌素类药物氯洁霉素等的原料
  • 灭火剂:二氧化碳、砂土、水、泡沫
  • 无气味。摩擦
  • 检测方法:GC
  • 参考质量标准:外观 白色结晶体 三苯基膦含量wt%≥99.7 三苯基氧膦含量wt%≤0.3 硫(S)PPM <5 氯(Cl)PPM <15 钠(Na)PPM <5 镁(Mg)PPM <5 铁(Fe)PPM <10 灰份PPM <100 干燥失重% <0.5 熔点℃ ≥78.5-81.5 溶解性 溶解于氯仿、乙酸和苯 4%四氯化碳溶液透光率%≥95
  • 急性毒性:口服-大鼠 LD50: 700 毫克/公斤; 口服-小鼠 LD50: 1000 毫克/公斤
  • 图谱信息:三苯基膦(603-35-0)Raman光谱 三苯基膦(603-35-0)红外图谱(IR1) 三苯基膦(603-35-0)红外图谱(IR2) 三苯基膦(603-35-0)红外图谱(IR3) 三苯基膦(603-35-0)核磁图( 13 CNMR) 三苯基膦(603-35-0)质谱(MS) 三苯基膦(603-35-0)核磁图( 1 HNMR)
  • 蒸气密度:9 (vs air)
  • 可燃性危险特性:受热分解有毒磷化物
  • {Chemica
  • 用途三:用于有机合成,聚合引发剂,抗菌素类药物氯洁霉素的原料,有机微量分析测定磷的标准样品。
  • Acros Organics:三苯基
  • 海关编码:29310095
  • 刺激数据:皮肤-兔子 500 毫克/24小时 重度; 眼睛-兔子 500 毫克/24小时 轻度
  • 蒸气压:5 mm H
  • 弗里德尔-克拉夫茨法:最佳反应条件:催化剂用量48g、反应时间8h、反应温度400℃,收率达63.5%。以硫、三氯化磷和苯直接回流反应,生成三苯基硫膦化合物,再 经铁粉还原得三苯基膦。
  • 储运特性:库房通风低温干燥; 与食品
  • 类别:有毒物品
  • 用途二:在农药上用于酯交换法合成有机磷中间体亚磷酸三甲酯,进而可得到敌敌畏、久效磷、磷胺等一系列有机磷杀虫剂,此外,它可用作合成橡胶和树脂的稳定剂、聚氯乙烯的抗氧剂,用作合成醇酸树脂和聚酯树脂的原料。
  • 下游产品:头孢克肟 --> 2-(二苯基膦基)乙胺 --> 齐多夫定 --> 5-苯基噻吩-2-羧酸 --> 硫酸长春地辛 --> 三苯基膦氯化钌 --> 2-二苯基膦-6-甲基吡啶 --> 反式-2-辛烯-1-醇 --> 5 5'-二甲基-2,2-联吡啶 --> 联萘二溴 --> N-(2-羟基乙基)-2-[4-(2-甲基丙基)苯基]丙酰胺 --> 3-溴异烟酸 --> 丁-3-炔-1-胺 --> 5-苯基-2-噻吩甲醛 --> (1-戊基)三苯基溴化磷 --> 二溴三苯基膦 --> 多虑平 --> 双(三苯基膦)氯化镍 --> 3-溴-2-吡啶羧酸 --> 拉西地平 --> 阿伐斯汀 --> 1,2-二(二苯基膦基)乙烷二氯化钯(II) --> N-BOC-6-溴代己胺 --> 异维 A 酸 --> 3-苯基吡唑 --> AE-活性酯 --> (甲氧基甲基)三苯基氯化 --> 乙基三苯基醋酸膦 --> 依维菌素 --> 甲基三苯基溴化
  • 方法一:其制备方法是以苯酚与三氯化磷为原料,经酯化反应后再经减压蒸馏,即得到产品亚磷酸三苯酯。 3C 6 H 5 OH+PCl 3 [15~20℃]→(C 3 H 5 O) 3 P+3HCl 具体工艺分间歇法和连续法两种。 (1)间歇法 将苯酚加入反应器中,温热熔化后加入三氯化磷,与苯酚在70~90℃开始反应,三氯化磷加完后,反应混合物温度将上升到150℃左右;在高温下减压除去溶解的氯化氢和未反应的苯酚,即得产品。 (2)采用塔式反应器 使苯酚从塔的上部冷凝器下方进入,三氯化磷从塔的下部接受器上方进入。二者在塔中进行反应,产物收集在接受器中,副产物氯化氢经冷凝器上端引入吸收塔。粗酯经蒸馏等处理即得产品。
  • 毒性分级:中毒

化学结构图

CAS 603-35-0  MFCD00003043
SMILES: c1ccc(P(C2CCCCC2)C2CCCCC2)cc1

化学属性

Mol. FormulaC18H15P
Mol. Weight262.29
Density1.132
Vapor Density9 (vs air)
Boiling Point377
Vapor Pressure5 mmHg ( 20 °C)
Melting Point79-81
Flash Point181°(358°F)
TSCAYes
SolubilitySoluble in ether, acetone, chloroform (50 mg/ml), and alcohol. Insoluble in water.
Stability对光敏感

别名和识别编码

Chemical NameTriphenylphosphine
MDL NumberMFCD00003043
CAS Number603-35-0
EC Number210-036-0
Beilstein Registry Number610776
Synonym
  • 三酚苯酯
  • TRIPHENYLPHOSPHINE, REAGENTPLUS, 99%
  • PP-360
  • Formylmethylene triphenylphosphorane
  • 三苯膦
  • 三苯基瞵
  • 瞵化三苯基
  • triphenyl-phosphin
  • Phosphorustriphenyl
  • Dehydrocholic acid CP2000
  • Trifenylfosfin
  • Triphenylphosphane
  • 三苯基膦
  • Trihenylphosphine
  • 三苯(基)磷
  • 三苯基膦, POWDER
  • Triphenylphosphine
  • TRP
  • phosphine,triphenyl
  • triphenyl-phosphane
  • 三苯基磷,三苯膦
  • Triphenylphosphide
  • TRIPHENYL PHOSPHOROUS
  • TRIPHENYLPHOSPHINE REAGENTPLUS(TM) 99%
  • Phosphine,triphenyl-
    Merck Number9743
    PubChem Substance ID 24900530
    Chemical Name Translation三苯基膦
    Reaxys-RN610776
    Wiswesser Line NotationRPR&R
    LabNetwork Molecule IDLN00198869

    系列性分类


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