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• {SNA} Analytical Standards, Analytical/Chromatography, Certified Reference Materials (CRMs), Chromatography, Fluka CRM for chromatography (neats), Organic CRMs Alphabetical, Organic CRMs TraceCERT, SVHC,
• {SNA} Alphabetical Index of Analytical Standards, Chemical Class, Alpha Sort, Analytical Standards, Analytical/Chromatography, Chloro, Chromatography, Environmental Standards, Halogenated, T, T-Z, TP - TZ, Volatiles/ Semivolatiles
• {SNA} Alkyl, Building Blocks, Chemical Synthesis, Halogenated Hydrocarbons, Organic Building Blocks
• {SNA} Additi

相关文献及参考

• Short: II/25C Title: Structure Data Of Free Polyatomic Molecules: Molecules containing Three or Four Carbon Atoms Author: Graner, G.; Hirota, E.; Iijima, T.; Kuchitsu, K.; Ramsay, D.A.; Vogt, J.; Vogt, N. Editor: Kuchitsu, K. Source: Landolt-Börnstein, New Series Volume: II/25C Year: 2001 Keyword: Free Polyatomic Molecules; Carbon Atoms; Molecules ISBN: 3-540-66774-1 ISBN: 978-3-540-66774-2 Internet Resource: DOI:10.1007/b71431 RefComment: VIII, 481 pages. Hardcover Abstract: This volume contains data on the geometric parameters (internuclear distances, bond angles, dihedral angles of internal rotation etc.) of free polyatomic molecules including free radicals and molecular ions. This survey on structure data is made of four subvolume, each containing the geometric parameters determined in the gas phase either by an analysis of the rotational constants (and sometimes the vibrational constants) obtained from microwave, infrared, Raman, electronic and photoelectron spectroscopy or by an analysis of electron diffraction intensities. Most of the structures listed in the tables are for molecules in the electronic ground state, but structures for electronically excited states have also been included as far as they are available. In this third subvolume, the structure of molecules containing three for four carbon atoms are listed.
• Short: III/20a Title: Nuclear Quadrupole Resonance Spectroscopy Data: Nuclei D ... Cl Author: Chihara, H.; Nakamura, N. Editor: Hellwege, K.-H.; Hellwege, A.M. Source: Landolt-Börnstein, New Series Volume: III/20a Year: 1988 Keyword: NQR ISBN: 3-540-18161-X ISBN: 978-3-540-18161-3 Internet Resource: DOI:10.1007/b31153 RefComment: IX,677 pages. Hardcover Abstract: Nuclear Quadrupole Resonance Spectroscopy has become a standard method for structural research in molecular and solid state physics as well as for different branches of chemistry. The volumes cover data for more than 8,000 substances in the solid state. Dat

安全信息

GHS Symbol

TYPE OF TEST            : TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - rat
DOSE/DURATION           : 5200 mg/kg/2Y-I
TOXIC EFFECTS :
   Tumorigenic - Carcinogenic by RTECS criteria
   Gastrointestinal - tumors
   Skin and Appendages - tumors
REFERENCE :
   NTPTR* National Toxicology Program Technical Report Series.  (Research
   Triangle Park, NC 27709) No.206-  Volume(issue)/page/year: NTP-TR-384,1993

TYPE OF TEST            : TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 3120 mg/kg/2Y-I
TOXIC EFFECTS :
   Tumorigenic - Carcinogenic by RTECS criteria
   Gastrointestinal - tumors
   Liver - tumors
REFERENCE :
   NTPTR* National Toxicology Program Technical Report Series.  (Research
   Triangle Park, NC 27709) No.206-  Volume(issue)/page/year: NTP-TR-384,1993

TYPE OF TEST            : LD50 - Let

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - guinea pig
DOSE/DURATION           : 340 mg/kg
TOXIC EFFECTS :
   Behavioral - somnolence (general depressed activity)
   Behavioral - ataxia
   Blood - other changes
REFERENCE :
   TKGMB8 Trudy Khar'kovskogo Meditsinskogo Instituta.  (Khar'kovskii
   Gosudarstvennyi Meditsinskii Institut, Kharkov, USSR) N.1- 1935-
   Volume(issue)/page/year: 124,27,1976

TYPE OF TEST            : LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Mammal - dog
DOSE/DURATION           : 200 mg/kg
TOXIC EFFECTS :
   Behavioral - sleep
   Liver - hepatitis (hepatocellular necrosis), zonal
   Liver - fatty liver degeneration
REFERENCE :
   AJHYA2 American Journal of Hygiene.  (Baltimore, MD)  V.1-80, 1921-64.  For
   publisher information, see AJEPAS.  Volume(issue)/page/year: 16,325,1932

TYPE OF TEST            : LC50 - Lethal concentration, 50 percent kill
ROUTE OF EXPOSURE       : Inhalation
SPECIES OBSERVED        : Rodent - mouse
DOSE/DURATION           : 3400 mg/m3/2H
TOXIC EFFECTS :
   Details of toxic effects not reported other than lethal dose value
REFERENCE :
   85GMAT "Toxicometric Parameters of Industrial Toxic Chemicals Under Single
   Exposure," Izmerov, N.F., et al., Moscow, Centre of International Projects,
   GKNT, 1982  Volume(issue)/page/year: -,114,1982

TYPE OF TEST            : LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - rabbit
DOSE/DURATION           : 380 mg/kg
TOXIC EFFECTS :
   Behavioral - somnolence (general depressed activity)
   Behavioral - ataxia
   Blood - other changes
REFERENCE :
   TKGMB8 Trudy Khar'kovskogo Meditsinskogo Instituta.  (Khar'kovskii
   Gosudarstvennyi Meditsinskii Instit

TYPE OF TEST            : Mutation in microorganisms
TEST SYSTEM             : Bacteria - Salmonella typhimurium
DOSE/DURATION           : 500 ng/plate
REFERENCE :
   ENMUDM Environmental Mutagenesis.  (New York, NY)  V.1-9, 1979-87.  For
   publisher information, see EMMUEG.  Volume(issue)/page/year: 7(Suppl
   3),15,1985

TYPE OF TEST            : DNA damage
ROUTE OF EXPOSURE       : Intraperitoneal
TEST SYSTEM             : Rodent - rat
DOSE/DURATION           : 55361 ug/kg
REFERENCE :
   CRTOEC Chemical Research in Toxicology.  (American Chemical Soc.,
   Distribution Office Dept. 223, POB 57/36, West End Station, Washington, DC
   20037)  V.1-    1988-  Volume(issue)/page/year: 4,528,1991

TYPE OF TEST            : Cytogenetic analysis
ROUTE OF EXPOSURE       : Inhalation
TEST SYSTEM             : Rodent - rat
DOSE/DURATION           : 800 ug/L
REFERENCE :
   BEXBAN Bulletin of Experimental Biology and Medicine (English Translation).
   Translation of BEBMAE. (Plenum Pub. Corp., 233 Spring St., New York, NY
   10013)  V.41-    1956-  Volume(issue)/page/year: 78,1414,1974

TYPE OF TEST            : DNA damage
TEST SYSTEM             : Human Lymphocyte
DOSE/DURATION           : 2 mmol/L
REFERENCE :
   MUREAV Mutation Research.  (Elsevier Science Pub. B.V., POB 211, 1000 AE
   Amsterdam, Netherlands) V.1-    1964-  Volume(issue)/page/year: 371,185,1996

TYPE OF TEST            : Sister chromatid exchange
TEST SYSTEM             : Rodent - hamster Lung
DOSE/DURATION           : 300 umol/L
REFERENCE :
   ENMUDM Environmental Mutagenesis.  (New York, NY)  V.1-9, 1979-87.  For
   publisher information, see EMMUEG.  Volume(issue)/page/year: 9,401,1987

TYPE OF TEST            : TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE       : Oral
SPECIES OBSERVED        : Rodent - rat
DOSE                    : 400 mg/kg
SEX/DURATION            : male 5 day(s) pre-mating
TOXIC EFFECTS :
   Reproductive - Fertility - litter size (e.g. # fetuses per litter; measured
   before birth)
REFERENCE :
   MUREAV Mutation Research.  (Elsevier Science Pub. B.V., POB 211, 1000 AE
   Amsterdam, Netherlands) V.1-    1964-  Volume(issue)/page/year: 101,321,1982

其他信息

• 下游产品:丙烯酰氯 --> 2,3-二氯丙烯
• 可燃性危险特性:受热分解;燃烧时产生有毒氯化物气体;与氧化剂起作用
• 毒性与危险情况:(1) 三氯丙烷有毒，有腐蚀性及刺激性，也能被皮肤吸收而中毒，蒸气有麻醉性，其作用和三氯甲烷相似，但较慢; 对眼睛和呼吸道有强刺激作用。大鼠经口LD50320 mg/kg。 (2) 易燃，燃点580℉(304℃)。空气中三氯丙烷的最高容许浓度美国为50ppm (300mg/m3)。
• 刺激数据:皮肤-兔子 700 毫克 轻度; 眼睛-兔子 140 毫克 重度
• 运输要求:三氯丙烷属有机易燃有毒品。危规号： 84007。运输时容器上须标有“易燃有毒品”标记。
• 测定方法:在空气中三氯丙烷的测定：用活性炭吸附，CS2处理，气相色谱法分析。
• Sigma Aldrich:96-18-4(sigmaaldrich)
• 爆炸物危险特性:与空气混合可爆
• 方法一:1.α-氯丙烯氯化法　丙烯高温氯化得烯丙基氯，经洗涤、分离后，再经低温氯化、分馏，即得成品。2.二氯异丙醇法。
• 用途一:用于生产农药和有机合成、气相色谱对比样品
• MOL 文件:96-18-4.mol
• 类别:有毒物品
• 图谱信息:1,2,3-三氯丙烷(96-18-4)核磁图( 13 CNMR) 1,2,3-三氯丙烷(96-18-4)红外图谱(IR1) 1,2,3-三氯丙烷(96-18-4)Raman光谱 1,2,3-三氯丙烷(96-18-4)核磁图( 1 HNMR) 1,2,3-三氯丙烷(96-18-4)质谱(MS)
• Alfa
• 海关编码:29031980
• 1,2,3-三氯丙烷价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2011/08/23 xp400276 三氯丙烷 5ml 300元 2011/04/16 S0655 1,2,3-三氯丙烷(1mg/ml的甲醇溶液)[用于水分析] 1,2,3-Trichloropropane (1mg/ml in Methanol) [for Water Analysis] 1ML 198元 2011/04/16 T0395 1,2,3-三氯
• 职业标准:TWA 300 毫克/立方米; STEL 450 毫克/立方米
• 挥发性有机化合物(VOCs)单组分标准液
• 用途二:主要用以生产1,2,3-三氯丙烯，也是一种较好的溶剂。亦可作农药矮壮素和燕麦敌的原料。
• 贮存:用塑料桶或铁桶盛装，防止机械性损坏。存放于阴凉、通风、干燥处，远离火源。
• 灭火剂:雾状水、泡沫、二氧化碳，干粉。
• 上游原料:丙烯酰氯 --> 1,3-二氯丙醇
• MSDS 信息:1,2,3-三氯丙烷(96-18-4).msds
• {Che
• TCI Shanghai:1,2,3-三氯丙烷(1mg/ml的甲醇溶液)[用于水分析] 1,2,3-Trichloropropane (1mg/ml in Methanol) [for
• Acros Organics:1,2,3-三氯丙烷 1,2,3-Trichloropropane, 99+ %(96-18-4)
• 有机合成中间体:三氯丙烷是一种重要有机合成中间体，可用于制备甘油、三氯丙烯、丙炔醇、三乙酸甘油酯、四氯丙烯、2-氯丙胺、多氯丙烷、2，4-二甲基-3-乙酰基呋喃；三氯丙烷也是生产农药原料，可用于生产农药矮壮素和燕麦敌。三氯丙烷也是一种较好的溶剂，清除金属表面涂料及油漆，亦用作油脂、蜡、树脂及氯化橡胶的溶剂。三氯丙烷与碱金属多硫化物、双二氯乙烯基缩甲醛缩聚生成ST型聚硫橡胶。此外三氯丙烷还用作色谱分析标准物质。 以上信息由Chemicalbook的彤彤编辑整理。
• 制备方法:(1) 从环氧氯丙烷生产中的高沸点混合物副产品中分离提取三氯丙烷。 (2) 以丙烯为原料进行氯化，可制得三氯丙烷。